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Experiment No. N

Analysis of Potassium Fluoride (KF)

Aim

To determine the presence of anion and cation in the given salt

Preliminary Test

  • Odor: Odorless
  • Texture: Crystalline
  • Color: White
  • Solubility: Soluble in water

Test of Anion

ExperimentObservationInference
Take the salt and treat with concentrated H₂SO₄Colourless gas evolves and it etches glassF⁻ may be present
Confirmatory Test
Calcium Chloride Test
Treat salt solution with calcium chloride solution
White gelatinous precipitate formsPresence of F⁻ is confirmed

Test of Cation

ExperimentObservationInference
Flame test in a clean non-luminous flameLilac flameK⁺ may be present
Confirmatory Test
Sodium Cobaltinitrite Test
Salt solution + sodium cobaltinitrite reagent
Yellow precipitateK⁺ is confirmed

Result

The given salt contains K⁺ ions as cation and F⁻ ions as anion. The salt is KF.

Precautions

  1. Handle the chemicals with care.
  2. Don't use excess of chemicals.
  3. Keep the mouth of the test tube away from the face.